Promazine_hydrochloride_LCMS_19117_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.DSample Name: BIZ2016-104-WJ3=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : P2-F-08Injection Date : 1/4/2016 2:15:37 PM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 6.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 1/4/2016 9:07:43 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 1/4/2016 2:23:32 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-B1225 Batch#19117 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.D) 1.686mAU1000800600400 2.292 2.475 1.532 2.59920000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.532 MM 0.0577 2.62951 7.59933e-1 0.0443 2 1.686 MM 0.0919 5927.70508 1074.88269 99.8758 3 2.292 MM 0.0468 1.55189 5.52611e-1 0.0261 4 2.475 MM 0.0580 1.86953 5.36907e-1 0.0315 5 2.599 MM 0.0535 1.31959 4.11088e-1 0.0222 Totals : 5935.07560 1077.14323 ===================================================================== *** End of Report ***HY-LCMS-02 1/4/2016 2:23:34 PM Yang Qian(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.DSample Name: BIZ2016-104-WJ3=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : P2-F-08Injection Date : 1/4/2016 2:15:37 PM Inj : 1 Inj Volume : 3.000 µlDifferent Inj Volume from Sample Entry Actual Inj Volume : 6.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 1/4/2016 9:07:43 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 1/4/2016 2:24:20 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-B1225 Batch#19117 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.D) ES-API, Pos, Scan 1.69770000060000050000040000030000020000010000000.511.522.53min HY-LCMS-02 1/4/2016 2:24:21 PM Yang Qian(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.DSample Name: BIZ2016-104-WJ3MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.697 7070544 286.20 I 285.20 I*MSD1 SPC, time=1.653:1.780 of D:\\AGLIENT 1260\\DATA\\20160104\\20160104 2016-01-04 09-07-43\\BIZ2016-104-WJ3.D ES-API, 1008060402002004006008001000m/z 285.2Max: 482392 *** End of Report ***HY-LCMS-02 1/4/2016 2:24:21 PM Yang Qian(LCMS-02) 287.2Page 2 of 2